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Okay, folks, here are the official instructions for making SIP's with Isoset. It ain't rocket science. Your best bet is building a vacuum tent the heavy vinyl-coated cloth. I'll post more information about how to build one of those shortly. Also, there are ways of applying the Isoset that don't involve purchasing a roll coater - these are very costly. One option I've considered would be to use a Wagner power roller -- you'd have to do some experiments to figure out how many grams of Isoset the pump pumps per second. If you started with a roller that's loaded with Isoset and you push the button to actuate the pump and then roll the roller in measured passes, you'd probably get a fairly uniform coating of Isoset.
I am not suggesting that people make these to sell... If you live in an area where there are no building codes and you don't need to insure your structure, this might be just the ticket for you.
More on vacuum tent design but in the meantime, here you go....
ISOSET ADHESIVE LAMINATING GUIDE FOR STRUCTURAL PANELS
INTRODUCTION: ISOSET is the leading adhesive for producing
structural panels. ISOSET WD3-A322
emulsion resin combined with ISOSET CX-47 crosslinker provides the east of
production, rapid and dependable production rates, and long-term durability
demanded by the structural panel industry.
TYPICAL MATERIALS USED:
Cores: Expanded or extruded polystyrene,
polyurethane, and
isocyanurate
foams or honeycomb.
Skins: Waferboard, oriented strandboard
(OSB), particleboard,
gypsum or
cementboard, and plywood.
Facings: Aluminum (backed or primed) and
fiberglass reinforced plastic
(FRP).
NOTE:
The mechanism for curing ISOSET adhesives is for water from the glueline
to be absorbed into one or both of the substrates being bonded during the
pressing time and the period of time after the stack has been removed from the
press and allowed to stand. After the
water is absorbed, the crosslinker reacts with the adhesive and crosslinks
it. Because of this requirement, direct
foam to metal or foam to plastic laminations cannot be made with ISOSET
adhesives because the foam is not porous enough to allow complete absorption of
the water from the glueline.
SAFETY AND HANDLING: Workers should wear proper gloves and eye
protection while mixing the adhesive.
Gloves are also recommended for workers handling the adhesive coated
panels. Consult Ashland’s
Material Safety Data Sheets for health, safety and handling information before
using these products.
MIXING INFORMATION: Add 16.7 parts by weight of ISOSET CX-47
crosslinker to 100 parts of ISOSET WD3-A322 resin emulsion. Other ISOSET emulsions and crosslinkers are
available. Contact your Ashland representative for more information.
Mix slowly until the
brown streaks caused by the addition of crosslinker disappear and a uniform tan
color is obtained (3 minutes maximum).
Avoid overmixing. Because of
limited pot life, batch size should match the use rate. Pot life is dependent on temperature; at 70°F
a pot life of 120 minutes can be expected.
At temperatures above 90°F, guard against dry-out on the roll coater.
GLUE SPREADER: The roll grooving for minimum squeeze-out
should be 14 x ½ grooves/inch composite (Black Brothers Code A2137). Wet rollers with water before placing glue on
the spreader to facilitate cleanup.
SPREAD RATE: To establish the spread rate, weigh a 1
Sq.Ft. piece of substrate. Fill the
bottom nip of the roll coater and run the test piece through the coater. After the correct weight has been
established, fill the top nip and run additional test pieces through until the
correct weight for both sides is established.
Avoid rollback of the adhesive on the test piece, since this will give a
false high reading for spread rate.
Recommended
coating weights for the various composites are as follows:
Construction
|
Spread Rate
|
Coating Weight
1 Sq.Ft. Test Piece
|
Skins
to Foam Core
·
Expanded Polystyrene 1 pcf
|
50-55 lbs/1000 ft2
|
23-25 grams
|
·
Isocyanurate 1.5 pcf
|
45-50 lbs/1000 ft2
|
21-23 grams
|
·
Extruded Polystyrene 2 pcf
|
45-50 lbs/1000 ft2
|
21-23 grams
|
·
Metal or FRP to Plywood 36 pcf
|
35-40 lbs/1000 ft2
|
16-18 grams
|
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Adjust
rollers until the correct spread rate is obtained. At warm temperatures, (>80°F), it will be
necessary to increase spread rate to maintain a 25 minute stack time. At cooler temperatures or shorter assembly
times, lower spread rates are possible.
ASSEMBLY TIME (STACK TIME): Once the laminating of the structural panels
has started, the maximum time before placing the stack of panels under pressure
is 30 minutes. Allow 25 minutes to build
the stack and 5 minutes to place the stack in the press and put it under pressure. This applies to ambient temperatures of
65°F-75°F. Higher temperatures will
cause dry-out and require a higher spread rate or shorter assembly time. When bonding OSB or waferboard, the panel
temperature should be between 55°F and 80°F.
Keep the open assembly time, when the glueline is fully exposed to the
air, below 1 minute.
PRESSURE: The recommended amount of pressure needed to
bond foam core panels is dependent on the type, density and thickness tolerance
of the foam. Some initial compression of
the foam is desirable, however, compression set should be avoided. As a general guide use:
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Core
|
Density
|
Pressure
|
Expanded
Polystyrene
|
1.0 pcf
|
5-7 psi
|
Isocyanurate
|
1.5 pcf
|
12-14 psi
|
Extruded
Polystyrene
|
2.0 pcf
|
35-40 psi
|
Plywood
|
36 pcf
|
40-50 psi
|
If
the adhesive spread rate and pressure are correct, small beads of squeeze-out
should be observed around the perimeter of each panel.
When
using a vacuum bag press for the higher density foams, the tolerances of the
foam must be good to obtain intimate contact all over the panel; maximum
available pressure must be used.
LAMINATING FACE MATERIALS: The recommended pressure for laminating FRP
or metal to OSB or waferboard is 40 psi if done in a separate step. It is possible to make foam core panels with
FRP or metal to wood facings in one step if the foam core can withstand higher
pressure. Successful 5-ply laminations
have been made in one step at 10 psi pressure.
Check the foam to be sure that 10 psi pressure does not initiate
compression set. The recommended press
times for various core materials are as follows:
Foam Core
|
Press Time
|
Expanded
Polystyrene
|
45 minutes
|
Isocyanurate
|
60 minutes
|
Extruded
Polystyrene
|
60 minutes
|
Do not laminate at temperatures below 55°F, measured at the
glueline. Add 15 minutes to the above
between 55°F and 60°F.
DRY-OUT: If there is
a break in the laminating operation for more than 30 minutes, such as during
lunch, pour a small amount of water (4 oz.) over each roller to prevent
dry-out. Too much water will alter bond
performance and cause delamination. Do
not allow adhesive to dry on the rollers.
If this occurs, cleanup is difficult.
When temperature exceeds 80°F, the cure cycle of the
adhesive shortens. Therefore, watch the
adhesive on the rollers closely for premature dry-out. Dry-out can be minimized by keeping the
rollcoater nip full of adhesive.
PROCESSING
INTERACTIONS: Be aware of the
interrelationship between spread rate,
moisture content of the skin, assembly time, temperature and press
time. For example, with a shorter assembly
time (e.g. 15 min.), lower spread rates may be used. Conversely, for longer assembly times, a
higher spread rate may be required.
Higher moisture content skins may require lower spread rates and longer
press times. The absorbency of the
substrates also influences these variables.
Contact your Ashland Technical
Representative for specific processing parameters at your facility.
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CLEAN-UP: Follow the clean-up procedures recommended by
the rollcoater manufacturer. Warm water
(100°F) makes clean-up easier. The use of Thermaclean1 resin
emulsifier helps reduce cleaning time.
Thoroughly clean rolls, troughs, and in and out feed areas.
Release coatings can facilitate clean-up of metal
surfaces. The use of Bates Boothcoating2
or Product No. 6273 has been successful
1Trademark, Cook Composites & Polymers, Heath, OH;
Phone: (614) 929-2866
2Trademark, U.S. Coatings Corporation, Buffalo, NY;
Phone: (716) 833-9366
3Trademark, Associated Chemists, Portland, OR;
Phone: (503) 659-1708
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